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As per IP 31 the apparatus consists of brass sleeve and case with metal cup and a glass boiling tube with cork fitted to a bath 600 ml beaker is provided. The assembly is kept on heater with energy regulator control and stand with F.H.P. elect. Stirrer. As per IP 132 the unit comprises a glass beaker with fiber cover together with glass test tube with three identifications to receive chromium plated brass cup. Cork for tube and a 1.5 mm diameter brass rod. The assembly is kept on heater with energy regulator and stand with F.H.P. motor stirrer.